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Hydrochloric Acid → 10-Phenacyl-2,3,4,10-tetrahydropyrimidino[1,2-a]benzimidazole hydrochloride

HRID 54706
Notes
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Reaction equation

HRID 54706 reaction equation
[CH2:1]([N:10]1[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[N:12]2[CH2:19][CH2:20][CH2:21][N:22]=[C:11]12)[C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[O:3].[ClH:23]>CC(C)=O>[ClH:23].[CH2:1]([N:10]1[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[N:12]2[CH2:19][CH2:20][CH2:21][N:22]=[C:11]12)[C:2]([C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1)=[O:3]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 791781HCID 791781, compound

Product 1

HCID 4488926310-Phenacyl-2,3,4,10-tetrahydropyrimidino[1,2-a]benzimidazole hydrochloride

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

The compound obtained in Step C is dissolved in acetone. The solution obtained is treated with concentrated hydrochloric acid. Suction-filter the precipitate and recrystallise from ethanol.

Workup

  1. custom
On this pageParticipantsProcedureWorkupSources & evidenceReaction notes
The solution obtained
  • filtrationSuction-filter the precipitate
  • customrecrystallise from ethanol
  • Sources & evidence

    ORD record
    ord-351a4862d0c74300aa0a29ea503c2b60
    Source dataset
    uspto-grants-1997_04
    DOI
    10.6084/m9.figshare.5104873.v1
    Patent number
    US05623073

    Reaction notes

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