3-Nonanone → HCID 72599204, compound

HRID 566319

Reaction equation

HRID 566319 reaction equation
[CH3:1][CH2:2][C:3](=O)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])(=[O:14])[NH:12][NH2:13]>C1CCCCC1>[CH2:2]([C:3](=[N:13][NH:12][C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])=[O:14])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:1]

Participants

4

Reactant 2

HCID 612353-NonanoneHCID 70091tert-Butyl carbazate

Product 1

HCID 72599204HCID 72599204, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

16.42 g (115 mmol) of 3-nonanone and 15.26 g (115.4 mmol) of tert-butyl carbazate are refluxed for 3 hours in 200 ml of cyclohexane. The solvent is removed in vacuo. This gives 30.54 g (product contains water) of a white solid, Rf=0.49 (cyclohexane/ethyl acetate=3:1).

Workup

  1. customThe solvent is removed in vacuo

Sources & evidence

ORD record
ord-44ffbfeb61be4a119fd1fc00e4af78ea
Source dataset
uspto-grants-2001_01
Patent number
US06174884B1

Linked notes

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