Trichloroethanol → HCID 49869898, compound

HRID 57206

Reaction equation

HRID 57206 reaction equation
[CH2:1]([O:15][C:16]1[O:20][C:19]([C:21]([OH:23])=[O:22])=[CH:18][CH:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Cl:24][C:25]([Cl:29])([Cl:28])[CH2:26]O>>[CH2:1]([O:15][C:16]1[O:20][C:19]([C:21]([O:23][CH2:26][C:25]([Cl:29])([Cl:28])[Cl:24])=[O:22])=[CH:18][CH:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

3

Reactant 2

HCID 8259TrichloroethanolHCID 1151755-(Tetradecyloxy)-2-furoic acid

Product 1

HCID 49869898HCID 49869898, compound

Procedure

The title compound was prepared as described in Example 1 starting from 0.228 g (0.7 mmol) of 5-(tetradecyloxy)furan-2-carboxylic acid and 0.196 mL (2.04 mmol) of 2,2,2-trichloroethanol. 1H NMR (400 MHz, DMSO-d6) δ: 7.4 (d, 1H), 5.74 (d, 1H), 5.03 (s, 2H), 4.19 (t, 2H), 1.7 (p, 2H), 1.2-1.5 (m, 22H), 0.85 (t, 3H).

Sources & evidence

ORD record
ord-9db678fdae484c24a8e2fa052365a9ff
Source dataset
uspto-grants-2016_09
Patent number
US09434718B2

Linked notes

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