1,2-Bis(2-chloroethoxy)ethane → HCID 15918510, compound

HRID 580307

Reaction equation

HRID 580307 reaction equation
[SH:1][CH2:2][CH2:3][S:4][CH2:5][CH2:6][SH:7].Cl[CH2:9][CH2:10][O:11][CH2:12][CH2:13][O:14][CH2:15][CH2:16]Cl.C(=O)([O-])[O-].[Cs+].[Cs+]>CN(C)C=O>[O:11]1[CH2:10][CH2:9][S:7][CH2:6][CH2:5][S:4][CH2:3][CH2:2][S:1][CH2:16][CH2:15][O:14][CH2:13][CH2:12]1

Participants

5

Reactant 3

HCID 81711,2-Bis(2-chloroethoxy)ethaneHCID 10796Cesium carbonateHCID 77117Bis(2-mercaptoethyl) sulfide

Product 1

HCID 15918510HCID 15918510, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

This compound is obtained by reacting 1,5-dimercapto-3-thiapentane with 1,8-dichloro-3,6-dioxaoctane in the presence of cesium carbonate in dimethylformamide (DMF): ##STR2##

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-9a9f2e69e5d948aa98b3cb162011c307
Source dataset
uspto-grants-1988_06
Patent number
US04752560

Linked notes

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