Diethyl Sulfate → HCID 59419919, compound

Reaction equation

[CH2:1]([O:3][C:4](=[O:16])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][CH3:15])[CH:7]=1)[CH3:2].COC1C=[C:21]([CH2:27][C:28]#N)C=CC=1OC.S(O[CH2:37][CH3:38])(OCC)(=O)=O.[Br:39]C(C)C>>[Br:39][CH2:28][CH2:27][CH2:21][C:5]([C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][CH3:15])[CH:7]=1)([CH2:37][CH3:38])[C:4]([O:3][CH2:1][CH3:2])=[O:16]

Participants

Reactant 4

HCID 6163Diethyl Sulfate

HCID 63582-Bromopropane

HCID 667273,4-Dimethoxybenzeneacetonitrile

HCID 87441Ethyl 3,4-dimethoxyphenylacetate

Product 1

HCID 59419919HCID 59419919, compound

Procedure

For Step 1, (3,4-dimethoxy-phenyl)-acetic acid ethyl ester was substituted for (3,4-Dimethoxyphenyl)acetonitrile and diethyl sulfate was substituted for 2-bromopropane.

Sources & evidence

ORD record: ord-17282a173cdb42e3b6bc42ba87783dc9
Source dataset: uspto-grants-2016_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09227918B2

Reaction notes

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