Methyl Methacrylate → Methyl 3-methoxyisobutyrate

HRID 591118

Reaction equation

HRID 591118 reaction equation
Cl[C:2]([CH3:8])([CH3:7])[C:3]([O:5][CH3:6])=[O:4].[C:9](OC)(=[O:13])C(C)=C>>[CH3:9][O:13][CH2:7][CH:2]([CH3:8])[C:3]([O:5][CH3:6])=[O:4]

Participants

3

Reactant 2

HCID 6658Methyl MethacrylateHCID 211144Methyl 2-chloro-2-methylpropanoate

Product 1

HCID 107177Methyl 3-methoxyisobutyrateYield 18%

Procedure

An analysis of the obtained crude reaction solution by gas chromatography revealed that the conversion of methyl 2-chloro-2-methylpropanoate was 68.8% and the yield of methyl methacrylate was 13.6%. As to another product, methyl 3-methoxy-2-methylpropanoate was obtained in an 18.0% yield.

Workup

  1. customAn analysis of the obtained crude
  2. customreaction solution by gas chromatography

Sources & evidence

ORD record
ord-88b2f0731aa84208bdaefca78bda6f6a
Source dataset
uspto-grants-2016_01
Patent number
US09238612B2

Linked notes

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