Butyl bromide → HCID 86592116, compound

HRID 601134

Reaction equation

[NH:1]1[C:6]2N=[CH:8][CH:9]=[CH:10][C:5]=2[C:4](=[O:11])[O:3][C:2]1=[O:12].[CH3:13][C:14]1[S:15][C:16]([CH2:19]Cl)=[CH:17][N:18]=1.[CH2:21](Br)CCC>>[CH3:13][C:14]1[S:15][C:16]([CH2:19][N:1]2[C:6]3[CH:21]=[CH:8][CH:9]=[CH:10][C:5]=3[C:4](=[O:11])[O:3][C:2]2=[O:12])=[CH:17][N:18]=1

Participants

Reactant 3

HCID 8002Butyl bromide

HCID 109865821H-Pyrido[2,3-d][1,3]oxazine-2,4-dione

HCID 128087945-(Chloromethyl)-2-methyl-1,3-thiazole

Product 1

HCID 86592116HCID 86592116, compound

Procedure

The title compound was prepared according to the procedure of Example 1B substituting isatoic anhydride for the product of Example 1A and 2-methyl-5-chloromethylthiazole for n-butyl bromide to give (0.410 g, 73%).

Workup

customto give (0.410 g, 73%)

Sources & evidence

ORD record: ord-304e0efdc0de4fa8802ad510bc4c0ab3
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07902203B2

Linked notes

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