Dimethylamine, hydrochloride → HCID 178457154, compound

HRID 605503

Reaction equation

[I-:1].[I-].[I-].[CH2:4]([N:7]([C:11]1[CH:12]=[CH:13][C:14]2[C:23]([CH:24]=1)=[S+:22][C:21]1[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=1)[N:15]=2)[CH2:8][CH2:9][CH3:10])[CH2:5][CH3:6].[CH2:25]([N:28](C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)[CH2:29]CC)CC.C(N(C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)CCC)CC.Cl.CNC>>[I-:1].[CH3:25][N:28]([C:19]1[CH:18]=[CH:17][C:16]2[C:21]([CH:20]=1)=[S+:22][C:23]1[C:14](=[CH:13][CH:12]=[C:11]([N:7]([CH2:8][CH2:9][CH3:10])[CH2:4][CH2:5][CH3:6])[CH:24]=1)[N:15]=2)[CH3:29]

Participants

Reactant 2

HCID 10473Dimethylamine, hydrochloride

HCID 178457153HCID 178457153, compound

Product 1

HCID 178457154HCID 178457154, compound

Procedure

This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with dimethylamine hydrochloride. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C20H26N3OS requires m/z=340; found m/z=340 (I− not detected by mass spectrometry).

Workup

customThis compound was obtained
customPrecipitation from dichloromethane
additionby addition of diethyl ether yielded purple lustrous crystals

Sources & evidence

ORD record: ord-abb8ea9582744c8aa4e3e8ef9b48faea
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07915254B2

Linked notes

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