N-Methylacetamide → methylvinyldi-(N-methylacetamido)silane
Reaction equation
[Na].[CH3:2][NH:3][C:4](=[O:6])[CH3:5].[CH3:7][CH:8]=[CH:9][SiH:10](Cl)Cl>C1(C)C=CC=CC=1>[CH3:7][CH:8]=[CH:9][SiH:10]([N:3]([CH3:2])[C:4](=[O:6])[CH3:5])[N:3]([CH3:2])[C:4](=[O:6])[CH3:5]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
The amidosilanes can be prepared as by the following illustration: mixing a sodium salt of N-methylacetamide with methylvinyldichlorosilane in an inert organic solvent such as toluene, filtering the by-produced sodium chloride from the toluene-product solution, and thereafter removing the toluene by vacuum distillation to obtain the product, methylvinyldi(N-methylacetamido)silane.
Workup
- filtrationfiltering the by-produced sodium chloride from the toluene-product solution
- customremoving the toluene
- distillationby vacuum distillation
Sources & evidence
- ORD record
- ord-7d66cc75a8fd414a9155bf2f7fa6be3b
- Source dataset
- uspto-grants-1993_09
- Patent number
- US05246980
Reaction notes
Loading…