HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-nitrobenzene → 1,3-Bis(4-nitrophenoxy)-2,2,4-trimethylpentane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| Reactant | 2,2,4-Trimethyl-1,3-pentanediol | HCID 8946 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 1,3-Bis(4-nitrophenoxy)-2,2,4-trimethylpentane | HCID 19860678 | — |
Reaction Steps
146 g (1 mol) 2,2,4-trimethyl-1,3-dihydroxypentane, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted using the same procedure described in Example 1 in 600 ml DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820866 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-81048ea7faf3483092d2da47a242376d |
| Source note | uspto-grants-1989_04 |