Reaction equation
[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8](Cl)=[O:9])(=[O:3])[CH3:2].[K].[CH3:15][S:16]([CH3:19])(=[NH:18])=[O:17]>O1CCCC1>[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8]([N:18]=[S:16]([CH3:19])([CH3:15])=[O:17])=[O:9])(=[O:3])[CH3:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- -35 °C
Procedure
A solution of 99.3 g of m-acetoxybenzoyl chloride in 150 ml of absolute tetrahydrofuran is added dropwise at -35° C. during 20 minutes while stirring to the dimethyl sulphoximine potassium salt suspension and the mixture is then stirred at -35° C. for 30 minutes. N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine is thus formed in suspension.
Sources & evidence
- ORD record
- ord-7abe3c7ad9e0455ab3840a266774c0b4
- Source dataset
- uspto-grants-1985_12
- Patent number
- US04556413
Linked notes
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