Reaction equation
O.O.O.O.O.O.O.O.O.[N+:10]([O-:13])([O-:12])=[O:11].[Al+3:14].[N+:15]([O-:18])([O-:17])=[O:16].[N+:19]([O-:22])([O-:21])=[O:20]>O>[N+:10]([O-:13])([O-:12])=[O:11].[Al+3:14].[N+:15]([O-:18])([O-:17])=[O:16].[N+:19]([O-:22])([O-:21])=[O:20]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
375.13 g (1 mole) of aluminum nitrate nonahydrate (Al(NO3)3.9H2O)(manufactured by Kansai Catalyst Co., Ltd., reagent grade, appearance: powder) was dissolved in water to obtain 1000 cm3 of an aluminum nitrate solution. 100 cm3 of the aluminum nitrate solution was added with 2.83 g of seed crystal described above (0.566 g in terms of Al2O3) to obtain a mixture. Then water was evaporated from the mixture under conditions of 75° C. by using a pressure-reduced drier, to obtain a powder. The amount of the seed crystal in terms of Al2O3 was 10 parts by weight per 100 parts by weight of the powder.
Sources & evidence
- ORD record
- ord-735f1f581498461dbdaff74b2d3091a4
- Source dataset
- uspto-grants-2010_04
- Patent number
- US07691362B2
Linked notes
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