Hydrochloric Acid → 1,1-Cyclopentanedimethanamine

HRID 653082

Reaction equation

HRID 653082 reaction equation
Cl.Cl.[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1.Cl>[OH-].[Na+].Cl[Pt-2](Cl)(Cl)Cl.[K+].[K+]>[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 1317151911,1-Cyclopentanedimethanamine, dihydrochloride

Product 1

HCID 4325931,1-Cyclopentanedimethanamine

Reagents, catalysts & solvents 2

HCID 61440Dipotassium tetrachloroplatinateCatalystHCID 14798Sodium HydroxideSolvent

Procedure

A 2.01 g portion of this amine derivative was dissolved in 20 ml of 1N sodium hydroxide, the pH was adjusted to 7.0 with hydrochloric acid and 4.15 g of potassium tetrachloroplatinate was added. The mixture was stirred for 4 hours, then the solid was collected, washed with water and dried, giving 2.1 g of 1,1-cyclopentanedimethanamine, compound with platinum chloride.

Workup

  1. additionwas added
  2. customthe solid was collected
  3. washwashed with water
  4. customdried

Sources & evidence

ORD record
ord-41bbad65c107481ba8ca2d3a2e78c1a2
Source dataset
uspto-grants-1987_06
Patent number
US04675336

Linked notes

Loading…