Dibutyl carbonate → Butyl 2,3-dihydroxypropylcarbamate

HRID 653507Notes

Reaction equation

C(O[C:6](=[O:12])[O:7][CH2:8][CH2:9][CH2:10][CH3:11])CCC.[NH2:13][CH2:14][CH:15]([OH:18])[CH2:16][OH:17]>>[OH:18][CH:15]([CH2:16][OH:17])[CH2:14][NH:13][C:6](=[O:12])[O:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

Reactant 2

HCID 68333Dibutyl carbonate

HCID 735613-Amino-1,2-propanediol

Product 1

HCID 20194878Butyl 2,3-dihydroxypropylcarbamate

Procedure

An equimolar mixture of dibutylcarbonate and 3-amino-1,2-propanediol was allowed to react resulting in formation of butyl 2,3-dihydroxypropylcarbamate.

Workup

customto react

Sources & evidence

ORD record: ord-9bffd8fdfd20489680067d2100400953
Source dataset: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04677168

Reaction notes

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