1-Butanol → 1,4-Cyclohexanedimethanol

HRID 653996Notes

Reaction equation

HRID 653996 reaction equation

[CH2:1]([OH:5])[CH2:2][CH2:3][CH3:4]>CC(C)[O-].CC(C)[O-].CC(C)[O-].CC(C)[O-].[Ti+4]>[CH:2]1([CH2:1][OH:5])[CH2:3][CH2:4][CH:2]([CH2:1][OH:5])[CH2:3][CH2:4]1

Participants

3

Reactant 1

HCID 2631-Butanol

Product 1

HCID 77351,4-Cyclohexanedimethanol

Reagents, catalysts & solvents 1

HCID 11026Titanium isopropoxideCatalyst

Procedure

20.09 g of titanium tetraisopropoxide in n-butanol (2.54 weight percent Ti)

Sources & evidence

ORD record: ord-22daa099c4da414e8ce419f12119dcc5
Source dataset: uspto-grants-1992_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05129947

Reaction notes

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