1-Chloro-4-nitrobenzene → 4-Nitrodiphenylamine

HRID 65489

Reaction equation

[N+:1]([C:4]1[CH:9]=[CH:8][C:7](Cl)=[CH:6][CH:5]=1)([O-:3])=[O:2].C([NH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=O>>[CH:17]1[CH:18]=[CH:19][C:14]([NH:13][C:7]2[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)=[CH:15][CH:16]=1

Participants

Reactant 2

HCID 74741-Chloro-4-nitrobenzene

HCID 7671Formanilide

Product 1

HCID 132714-Nitrodiphenylamine

Procedure

combining in a reaction zone paranitrochlorobenzene and a molar excess of formanilide at condensation temperature for forming 4-nitrodiphenylamine and

Sources & evidence

ORD record: ord-7e6b2f9ac7ab4ba1b438656e9132d395
Source dataset: uspto-grants-1986_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04614817

Linked notes

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