Dimethylethylamine → Dimethylethylammonium Trifluoromethanesulfonate

HRID 655089

Reaction equation

HRID 655089 reaction equation
[CH3:1][N:2]([CH3:5])[CH2:3][CH3:4].[F:6][C:7]([F:13])([F:12])[S:8]([OH:11])(=[O:10])=[O:9]>>[F:6][C:7]([F:13])([F:12])[S:8]([O-:11])(=[O:10])=[O:9].[CH3:1][NH+:2]([CH3:5])[CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 11723Dimethylethylamine2×HCID 62406Trifluoromethanesulfonic acid2×

Product 1

HCID 86620366Dimethylethylammonium Trifluoromethanesulfonate

Procedure

Equimolar amounts of dimethylethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed dimethylethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Workup

  1. temperaturewhile being cooled by liquid nitrogen
  2. customthus obtaining a target ionic conductor

Sources & evidence

ORD record
ord-07047aba1c4045b6a58f03f746e70f9c
Source dataset
uspto-grants-2011_12
Patent number
US08071253B2

Linked notes

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