3-Phenylprop-2-Enal → Cinnamylpiperazine

HRID 704392

Reaction equation

HRID 704392 reaction equation
[N:1]1([C:7](OCC)=O)[CH2:6][CH2:5][NH:4][CH2:3][CH2:2]1.C(=O)[CH:13]=[CH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH2:7]([N:1]1[CH2:2][CH2:3][NH:4][CH2:5][CH2:6]1)[CH:13]=[CH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 3073-Phenylprop-2-EnalHCID 84311-Piperazinecarboxylic acid, ethyl ester

Product 1

HCID 86803Cinnamylpiperazine

Procedure

Ethyl 1-piperazinecarboxylate and cinnamaldehyde were used as the starting materials and treated in the same ,manner as in Reference Example 51 to give 1-cinnamylpiperazine as an oil.

Workup

  1. additiontreated in the same ,manner as in Reference Example 51

Sources & evidence

ORD record
ord-e59f9c72e9f549a8a85f703088674ec7
Source dataset
uspto-grants-1991_01
Patent number
US04987132

Linked notes

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