HCID 178488187, compound → HCID 178488184, compound

HRID 722200Notes

Reaction equation

HRID 722200 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:12]2[NH:16][C:15]([CH3:17])=[N:14][N:13]=2)[CH:6]=[CH:7][C:8]=1[N+:9]([O-])=O>C1COCC1.[Pd]>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:12]2[NH:16][C:15]([CH3:17])=[N:14][N:13]=2)[CH:6]=[CH:7][C:8]=1[NH2:9]

Participants

4

Reactant 1

HCID 178488187HCID 178488187, compound

Product 1

HCID 178488184HCID 178488184, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8028TetrahydrofuranSolvent

Procedure

was prepared by hydrogenating 100 mg of 3-(3-methoxy-4-nitrophenyl)-5-methyl-4H-[1,2,4]triazole in the presence of Pd/C in THF and used further without further purification.

Workup

  1. customused further without further purification

Sources & evidence

ORD record
ord-c0e6c23daf4e456ebce6e3f37f07146d
Source dataset
uspto-grants-2006_11
Patent number
US07138414B2

Reaction notes

Loading…