HomeMCPWorkbenchSkills
HomeWorkbenchNotificationsMe
llms.txt · MCP GuidePrivacy Policy · Terms of Service · Supportv1.8.0
  1. Home
  2. /Reaction

Benzaldehyde → HCID 67136987, compound

HRID 723367
Notes
Print preview

Reaction equation

HRID 723367 reaction equation
[O:1]([C:8]1[CH:13]=[CH:12][C:11]([NH:14][NH2:15])=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:16](=O)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>CO>[CH:16](=[N:15][NH:14][C:11]1[CH:12]=[CH:13][C:8]([O:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[CH:9][CH:10]=1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 2760972(4-Phenoxyphenyl)hydrazine

Product 1

HCID 67136987HCID 67136987, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A suspension of (4-phenoxyphenyl)hydrazine (J. Org. Chem. 1956, 395; 1.5 g) in methanol (10 mL) was mixed with benzaldehyde (0.76 mL) and heated to reflux. The crystals which separated out on cooling were filtered off with suction. The product with the molecular weight of 288.35 (C19H16N2O); MS (ESI): 289 ([M+H]+), was obtained in this way.

Workup

temperature
heated to reflux
  • customThe crystals which separated out
  • temperatureon cooling
  • filtrationwere filtered off with suction
  • customMS (ESI): 289 ([M+H]+), was obtained in this way
  • Sources & evidence

    ORD record
    ord-559485146324438eaa0a475c3a734b00
    Source dataset
    uspto-grants-2006_11
    DOI
    10.6084/m9.figshare.5104873.v1
    Patent number
    US07141561B2

    Reaction notes

    Loading…

    On this pageParticipantsProcedureWorkupSources & evidenceReaction notes