Ethanol → Ethyl sulfoacetate

HRID 747777

Reaction equation

HRID 747777 reaction equation
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH2:9](O)[CH3:10]>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Participants

3

Reactant 2

HCID 702EthanolHCID 31257Sulfoacetic acid

Product 1

HCID 12216623Ethyl sulfoacetate

Conditions

Temperature
80 °C

Procedure

2.21 g (15.8 mmol) of sulfoacetic acid was suspended in 30 ml of ethanol, and the suspension was heated at 80° C. under reflux for 5 hours. The solvent was distilled off to obtain the title compound.

Workup

  1. temperatureunder reflux for 5 hours
  2. distillationThe solvent was distilled off

Sources & evidence

ORD record
ord-7c0ee0c177f14bd0af3e41d8c0c28fe5
Source dataset
uspto-grants-2008_07
Patent number
US07396844B1

Linked notes

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