Potassium Carbonate → HCID 22939443, compound
Reaction equation
C([O:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([C:14]#[N:15])[N:9]=1)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO>[OH:4][CH2:5][CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]#[N:15])[CH:11]=[CH:12][CH:13]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
3-(6-Cyano-2-pyridyl)propyl acetate (3.0 g, 14.7 mmol) was dissolved in methanol (15 ml), and potassium carbonate (0.08 g, 0.58 mmol) was added thereto. The reaction mixture was stirred at room temperature for 22 hrs and concentrated to give the titled compound (2.2 g, 92%).
Workup
- concentrationconcentrated
Sources & evidence
- ORD record
- ord-3ea673b917ad418ea742e738f8ee0f9e
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07399759B2
Reaction notes
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