HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(3-fluoro-4-methylphenyl)-2-isobutyl-4-methane-sulfonyloxymethyl-2H-pyridazin-3-one → 2-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(3-fluoro-4-methylphenyl)-2-isobutyl-4-methane-sulfonyloxymethyl-2H-pyridazin-3-one | HCID 21991531 | — |
| Reactant | 4-hydroxymethyl-2-isobutyl-6-phenyl-2H-pyridazin-3-one | HCID 21991628 | — |
| Product | 2-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one | HCID 21991562 | 68.4% |
Reaction Steps
Following the procedure of Example 1 (9), 4-hydroxymethyl-2-isobutyl-6-phenyl-2H-pyridazin-3-one was reacted to yield the title compound as colorless fine-needles (yield: 68.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087606B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-ac14e02261ea4cb49fe34891bbbfb985 |
| Source note | uspto-grants-2006_08 |