Reaction equation
[CH2:1]=[O:2].[C:3]1([CH:10]=[CH:9][CH:8]=[C:6]([OH:7])[CH:5]=1)[OH:4].[OH-].[Na+]>>[C:3]1([CH:10]=[CH:9][CH:8]=[C:6]([OH:7])[CH:5]=1)[OH:4].[CH2:1]=[O:2]Participants
4
Procedure
Formaldehyde in aqueous solution is added to the granules of resorcinol silicoformate acid in the ratio of about 1 to 1 mols. Sodium hydroxide is added until the pH is between 10 to 12. The mixture is then heated to 50° to 85° C while agitating and the resorcinol silicoformate goes into solution. In 30 to 90 minutes the reaction is complete, thereby producing a formaldehyde resorcinol silicoformate resinous compound. This compound is soluble in acetone and other organic solvents.
Workup
- temperatureThe mixture is then heated to 50° to 85° C
Sources & evidence
- ORD record
- ord-1b419760217246bfb5b8d0b275a3e7aa
- Source dataset
- uspto-grants-1978_06
- Patent number
- US04094825
Linked notes
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