Furfural → Furfural diurea silicate

Reaction equation

[CH:1](=[O:7])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[Si:8]([OH:12])([OH:11])([OH:10])[OH:9].[NH2:13][C:14]([NH2:16])=[O:15].[NH2:17][C:18]([NH2:20])=[O:19]>>[Si:8]([OH:12])([OH:11])([OH:10])[OH:9].[NH2:13][C:14]([NH2:16])=[O:15].[NH2:17][C:18]([NH2:20])=[O:19].[CH:1](=[O:7])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 7362Furfural2×

HCID 86734905Diurea silicate

Product 1

HCID 86735758Furfural diurea silicate

Procedure

About 2 mols of furfural are mixed with one mol of the diurea silicate and heated to just below the boiling temperature of furfural while agitating at ambient pressure for 20 to 120 minutes, until the desired viscosity is obtained, thereby producing poly (furfural diurea silicate) resinous product.

Workup

customuntil the desired viscosity is obtained

Sources & evidence

ORD record: ord-fe3e94a4239f42a1b3c3ae0a438ed879
Source dataset: uspto-grants-1978_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04096118

Reaction notes

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