2,6-Di-tert-butyl-4-mercaptophenol → HCID 14011803, compound
Reaction equation
[CH3:1][O:2][C:3](=[O:11])[CH2:4][S:5]([CH2:8][CH2:9]Cl)(=[O:7])=[O:6].[O-][CH2:13]C.[Na+].[CH3:16][C:17]([C:20]1[CH:25]=[C:24]([SH:26])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:19])[CH3:18]>>[CH2:1]([O:2][C:3](=[O:11])[CH2:4][S:5]([CH2:8][CH2:9][S:26][C:24]1[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]([OH:31])=[C:20]([C:17]([CH3:16])([CH3:18])[CH3:19])[CH:25]=1)(=[O:7])=[O:6])[CH3:13]Participants
4
Procedure
The title compound was prepared according to the method of Example 12 from the title compound of Example 16, sodium ethoxide and 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol, m.p. ca. 95° C.
Sources & evidence
- ORD record
- ord-d7475121e5c744678d776fa439027d92
- Source dataset
- uspto-grants-1988_07