Hydrochloric Acid → HCID 67167889, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[O:13]COC.Cl>CO.O1CCOCC1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[OH:13]Participants
5
Reactant 2
Product 1
Reagents, catalysts & solvents 2
Procedure
To a suspension of Example 383B in methanol (15 mL) was added 4 N HCl in dioxane (1 mL). The mixture was stirred for 4 hours, concentrated, and diluted with water. The precipitates were collected to afford the titled compound.
Workup
- concentrationconcentrated
- additiondiluted with water
- customThe precipitates were collected
Sources & evidence
- ORD record
- ord-eda001caede046d5b5e12f4a20bc9b01
- Source dataset
- uspto-grants-2014_09
- Patent number
- US08846951B2
Reaction notes
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