Ethyl 2-bromoisovalerate → HCID 178440514, compound
Reaction equation
[C:1]1([NH:7][C:8]([NH2:10])=[S:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH:12]([CH:18]([CH3:20])[CH3:19])[C:13](OCC)=[O:14]>>[NH:7]([C:8]1[S:9][CH:12]([CH:18]([CH3:20])[CH3:19])[C:13](=[O:14])[N:10]=1)[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
Synthesis was performed from N-phenylthiourea and ethyl 2-bromo-3-methylbutanoate according to Method C.
Workup
- customSynthesis
Sources & evidence
- ORD record
- ord-399833c9338c4eb5a3921febba2e2760
- Source dataset
- uspto-grants-2007_08
- Patent number
- US07253196B2
Reaction notes
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