Benzaldehyde → 4-(Benzylideneamino)benzenesulfonamide

Reaction equation

[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:9]([C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1)(=[O:12])(=[O:11])[NH2:10]>>[CH:1](=[N:17][C:16]1[CH:18]=[CH:19][C:13]([S:9](=[O:12])(=[O:11])[NH2:10])=[CH:14][CH:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 240Benzaldehyde

HCID 5333Sulfanilamide

Product 1

HCID 3084054-(Benzylideneamino)benzenesulfonamide

Procedure

Following a procedure similar to that described in Example 1(i), but using benzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 91%).

Sources & evidence

ORD record: ord-37c2de56b25442a0ae500d624b9431af
Source dataset: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE039420E1

Reaction notes

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