Allyl bromide → HCID 19702699, compound
Reaction equation
[OH:1][CH2:2][CH2:3][NH:4][C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][CH:6]=1.[CH2:14](Br)[CH:15]=[CH2:16]>CN1CCCC1=O>[CH2:16]([N:4]([CH2:3][CH2:2][OH:1])[C:5]1[CH:6]=[CH:7][C:8]([N+:11]([O-:13])=[O:12])=[CH:9][CH:10]=1)[CH:15]=[CH2:14]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
N-(2-hydroxyethyl)-4-nitrobenzenamine (9.1 g, 0.05 mol) is treated with allyl bromide in N-methylpyrrolidone, also as subsequently discussed in Example 11, to provide N-allyl-N-(2-hydroxyethyl)-4-nitrobenzenamine.
Sources & evidence
- ORD record
- ord-3a331c28066c45748e51f2493f64f9aa
- Source dataset
- uspto-grants-1998_02
- Patent number
- US05714304
Reaction notes
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