2-Ethylphenol → 2-Ethenylphenol

HRID 866812

Reaction equation

HRID 866812 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])[CH3:2].C(C1C=C(O)C=CC=1)C.C(C1C=CC(O)=CC=1)C>C1(C)C=CC=CC=1>[CH:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])=[CH2:2]

Participants

5

Reactant 3

HCID 69972-Ethylphenol2×HCID 121013-EthylphenolHCID 312424-Ethylphenol

Product 1

HCID 1354422-Ethenylphenol

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

As a result, 3.5 liters of a toluene solution containing 1.5 mols of a vinylphenol mixture of 37.0 mol% o-vinylphenol, 24.7 mol% m-vinylphenol, 36.9 mol% p-vinylphenol and 1.4 mol% ethylphenol was obtained as the extract. As the raffinate, 10.4 liters of a toluene solution containing 2.6 mols of an ethylphenol mixture of 9.9 mol% o-ethylphenol, 4.0 mol% m-ethylphenol, 85.1 mol% p-ethylphenol and 1.0 mol% vinylphenol was obtained.

Sources & evidence

ORD record
ord-29ddc7589a894f019fc69d882c6627f7
Source dataset
uspto-grants-1978_07
Patent number
US04101590

Linked notes

Loading…