Hydrogen Peroxide → Titanium Borate

HRID 883444

Reaction equation

HRID 883444 reaction equation
[B:1]([OH:4])([O-:3])[O-:2].[B:5]([OH:8])([OH:7])[OH:6].[B:9]([OH:12])([OH:11])[OH:10].[B:13]([OH:16])([OH:15])[OH:14].[Na+].[Na+].[Ti:19].OO>O>[B:1]([O-:4])([O-:3])[O-:2].[Ti+4:19].[B:5]([O-:8])([O-:7])[O-:6].[B:9]([O-:12])([O-:11])[O-:10].[B:13]([O-:16])([O-:15])[O-:14].[Ti+4:19].[Ti+4:19]

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 23963TitaniumHCID 86623386Disodium;boric acid;hydrogen borate

Product 1

HCID 86623385Titanium Borate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

200 g of disodium tetraborate was dissolved in 800 ml of hot deionized water. The water is in the temperature range of about 85° C. to about 95° C. 150 g of 45% titanium III sulfate was added to the above solution to form a dark slurry. 35% H2O2 was added drop-wise to the slurry until a homogenous yellow suspension resulted. The product was filtered in a Büchner funnel, and the cake was washed with deionized water. Solids were determined to be 19.8% by oven drying.

Workup

  1. customis in the temperature range of about 85° C. to about 95° C
  2. customto form a dark slurry
  3. customresulted
  4. filtrationThe product was filtered in a Büchner funnel
  5. washthe cake was washed with deionized water
  6. customdrying

Sources & evidence

ORD record
ord-b372d4d290414a72a32bff275504bd9d
Source dataset
uspto-grants-2012_08
Patent number
US08236884B2

Linked notes

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