N,N-Dimethylethylenediamine → HCID 178472135, compound
Reaction equation
[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][NH2:5].Cl.C(O[C:11](=[NH:18])[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14])C>C(O)C>[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][NH:5][C:11](=[NH:18])[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
To a solution of N,N-dimethyl-1,2-diaminoethane (8.8 g, 0.1 mmol) in absolute ethanol (40 ml) is added ethyl 3-ethoxy-3-iminopropionate hydrochloride (20.0 g, 0.1 mmol). After stirring at ambient temperature for 16 hours, evaporated solvent and dissolved residue in water, made basic with sodium carbonate and extracted product into methylene chloride. This solution is evaporated to dryness to give 17 g of crude viscous title A product.
Workup
- customevaporated solvent
- dissolutiondissolved residue in water
- extractionextracted product into methylene chloride
- customThis solution is evaporated to dryness
- customto give 17 g of crude viscous title A product
Sources & evidence
- ORD record
- ord-104e7d6420624e74a9b8cc94dc828240
- Source dataset
- uspto-grants-1983_12
- Patent number
- US04420615
Reaction notes
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