Bromoacetyl bromide → 5-(2-Bromoacetyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

HRID 959

Reaction equation

[O:1]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[NH:5][CH2:4][CH2:3][CH2:2]1.[Br:12][CH2:13][C:14](Br)=[O:15]>>[Br:12][CH2:13][C:14]([N:5]1[C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:1][CH2:2][CH2:3][CH2:4]1)=[O:15]

Participants

Reactant 2

HCID 61147Bromoacetyl bromide

HCID 5777522,3,4,5-Tetrahydro-1,5-benzoxazepine

Product 1

HCID 196942555-(2-Bromoacetyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

Procedure

2,3,4,5-tetrahydro-1,5-benzoxazepine [E. K. Orlova et al.; Kim. Geterotsikl. Soedin.,9, 1296 (1975): Chem. abstra., 84, 59411] and bromoacetyl bromide were used to produce the above compound in the same way as Reference Example 8.

Workup

customto produce the above compound in the same way as Reference Example 8

Sources & evidence

ORD record: ord-63a70aa1c69f4c69985323de9986a8eb
Source dataset: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05723475

Linked notes

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