4-Chlorobutyryl chloride → 5-(4-Chlorobutyryl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

HRID 960

Reaction equation

HRID 960 reaction equation
[O:1]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[NH:5][CH2:4][CH2:3][CH2:2]1.[Cl:12][CH2:13][CH2:14][CH2:15][C:16](Cl)=[O:17]>>[Cl:12][CH2:13][CH2:14][CH2:15][C:16]([N:5]1[C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:1][CH2:2][CH2:3][CH2:4]1)=[O:17]

Participants

3

Reactant 2

HCID 783704-Chlorobutyryl chlorideHCID 5777522,3,4,5-Tetrahydro-1,5-benzoxazepine

Product 1

HCID 196942505-(4-Chlorobutyryl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

Procedure

2,3,4,5-tetrahydro-1,5-benzoxazepine and 4-chlorobutyryl chloride were used to produce the above compound in the same way as Reference Example 8.

Workup

  1. customto produce the above compound in the same way as Reference Example 8

Sources & evidence

ORD record
ord-04e4aa0d550f42b3965842045af58c87
Source dataset
uspto-grants-1998_03
Patent number
US05723475

Linked notes

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