→ Methyl 4-(4-fluorophenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Reaction equation
CC(=O)O.CCO.COC(=O)CC(C)=O.NC(N)=O.O.O=Cc1ccc(F)cc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>COC(=O)C1=C(C)NC(=O)NC1c1ccc(F)cc1Participants
7
Reactant 0
No Reactant data yet.
Product 1
Reagents, catalysts & solvents 6
Conditions
- Temperature
- 120 °C
Workup
- waitNo procedure recorded
- filtrationKeep solid
- washNo procedure recorded
- dry in vacuumNo procedure recorded
Sources & evidence
- ORD record
- ord-00a1b82def01418299554ed7d2bfc2c5
- Source dataset
- Microwave-assisted Biginelli Condensation Dataset
- Original link
- View source
Reaction notes
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