→ HCID 110273790, compound

HRID 962344Notes

Reaction equation

HRID 962344 reaction equation
CC(=O)O.CCO.CNC(=O)CC(C)=O.NC(N)=O.O.O=Cc1ccccc1[N+](=O)[O-].O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CNC(=O)C1=C(C)NC(=O)NC1c1ccccc1[N+](=O)[O-]

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 110273790HCID 110273790, compoundYield 66%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 111012-NitrobenzaldehydeOtherHCID 88483N-MethylacetoacetamideOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-6c0f57dcfc334310a02c81d34d14c095
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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