HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperacillin → Piperacillin 2-acetamido-2-deoxy-N-(1-amino-(R/S)-dodecoyl)-beta-D-gluco-pyranosylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperacillin | HCID 43672 | — |
| Reactant | 2-acetamido-2-deoxy-N-(1-amino-(R/S)-dodecoyl)-beta-D-glucopyranosylamine | HCID 131726725 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Piperacillin 2-acetamido-2-deoxy-N-(1-amino-(R/S)-dodecoyl)-beta-D-gluco-pyranosylamine | HCID 131726724 | 97% |
Reaction Steps
Piperacillin (2.00 g, 3.87 mmol) and 2-acetamido-2-deoxy-N-(1-amino-(R/S)-dodecoyl)-β-D-glucopyranosylamine (32) (1.61 g, 3.87 mmol) were dissolved in 95% acetic acid. Once fully dissolved, the solution was filtered and lyophilised to give (35) as a white solid (3.50 g, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312194B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-687e629e145f4b0997f44d0314ac4f67 |
| Source note | uspto-grants-2007_12 |