Methyl Acrylate → HCID 53766522, compound

Reaction equation

[NH2:1][CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1.[C:9]([O:13][CH3:14])(=[O:12])[CH:10]=[CH2:11]>>[CH3:14][O:13][C:9]([CH2:10][CH2:11][N:1]([CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1)[CH2:11][CH2:10][C:9]([O:13][CH3:14])=[O:12])=[O:12]

Participants

Reactant 2

HCID 7294Methyl Acrylate

HCID 310183-Pyridinemethanamine

Product 1

HCID 53766522HCID 53766522, compound

Procedure

52.06 Grams of 3-aminomethylpyridine was refluxed with 200 milliliters of methyl acrylate for 96 hours. The excess methyl acrylate was evaporated off to give 137.6 grams of 3-[N,N-di(2-methoxycarbonylethyl)aminomethyl] pyridine.

Workup

customThe excess methyl acrylate was evaporated off

Sources & evidence

ORD record: ord-da7af07fcf8d44359b3ca5c50a1207c6
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04053615

Reaction notes

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