Diethylamine → N,N-Diethylmethanesulphonamide

HRID 974518

Reaction equation

[CH3:1][S:2](F)(=[O:4])=[O:3].[NH:6]([CH2:9][CH3:10])[CH2:7][CH3:8]>>[CH3:1][S:2]([N:6]([CH2:9][CH3:10])[CH2:7][CH3:8])(=[O:4])=[O:3]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 11207Methanesulfonyl Fluoride

Product 1

HCID 75411N,N-DiethylmethanesulphonamideYield 96.5%

Procedure

Chem. Abstracts 56:7116f, abstracting Sokolsku et al., Izvest. Akad Nauk S.S.S.R., Otdel Khem Nauk 1606 (1968), describes the reaction of CH3SO2F with (C2H5)2NH after one day to give 96.5% CH3SO2N(C2H5)2.

Sources & evidence

ORD record: ord-cd4deffa199c4130b764a010db21a5f5
Source dataset: uspto-grants-1991_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05068427

Linked notes

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