HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Allyl-N-(1,1-dimethoxyprop-2-yl)-urethane → Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Allyl-N-(1,1-dimethoxyprop-2-yl)-urethane | HCID 15069988 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate | HCID 15069993 | — |
Reaction Steps
76.5 g (0.213 mol) of 64.5% pure N-allyl-N-(1,1-dimethoxyprop-2-yl)-urethane are heated in 180 ml of formic acid at 100° C. for one hour. The mixture is poured into ice-water and extracted with CH2Cl2, the extracts are washed neutral with NaHCO3 solution, dried over MgSO4 and concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05607942 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-0457777cb6f44f7787d9c40a78e8996c |
| Source note | uspto-grants-1997_03 |