Triphenylphosphine → HCID 19965615, compound

Reaction equation

[Cl:1][CH2:2][C:3]1[N:4]=[C:5]([C:9]2[O:10][CH:11]=[CH:12][CH:13]=2)[O:6][C:7]=1[CH3:8].[C:14]1([P:20]([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[Cl-:1].[O:10]1[CH:11]=[CH:12][CH:13]=[C:9]1[C:5]1[O:6][C:7]([CH3:8])=[C:3]([CH2:2][P+:20]([C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)[N:4]=1

Participants

Reactant 2

HCID 11776Triphenylphosphine

HCID 223445824-(Chloromethyl)-2-(furan-2-yl)-5-methyl-1,3-oxazole

Product 1

HCID 19965615HCID 19965615, compound

Procedure

4-Chloromethyl-2-(2-furyl)-5-methyloxazole and triphenylphosphine were reacted in the same manner as in Reference Example 7 to yield [2-(2-furyl)-5-methyl-4-oxazolylmethyl]triphenylphosphonium chloride. Melting point 284°-285° C.

Sources & evidence

ORD record: ord-6b088d0bd9314a9cb73cbbbbfded068d
Source dataset: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05614544

Reaction notes

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