HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Acetic Acid 12-(4-Formyl-phenoxy)-dodecyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-(12-Hydroxy-dodecyloxy)-benzaldehyde | HCID 22987548 | — |
| Product | Acetic Acid 12-(4-Formyl-phenoxy)-dodecyl Ester | HCID 11244987 | — |
Reaction Steps
4-(12-Hydroxyl-dodecyloxy)-benzaldehyde (1.1 g, 3.6 mmol, see Example 2 above) was heated at reflux in acetic anhydride (15 ml) for 90 minutes. After cooling, the solution was poured into water with stirring. The title compound formed as a precipitate which was collected by filtration, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630128B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-f8fc0837b3a749fabb70322c2da38585 |
| Source note | uspto-grants-2003_10 |