化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 2,6-Di-tert-butyl-4-(methoxymethyl)phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Butylated hydroxymethylphenol | HCID 6929 | — |
| 触媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | 2,6-Di-tert-butyl-4-(methoxymethyl)phenol | HCID 6911 | 94% |
反応手順
A solution of 4-hydroxymethyl-2,6-di-t-butylphenol (0.5 g) in methanol (10 mL) containing 1 drop of concentrated hydrochloric acid was stirred at ambient temperature for 1 hour. Evaporation of the solvent gave the title compound, 0.5 g, 94% yield as a white crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06048995 |
| 出典データセット | uspto-grants-2000_04 |
| ORD ID | ord-113efb57cef44a829e4e591636f562cf |
| 出典メモ | uspto-grants-2000_04 |