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HRID1004437

反应详情

EQUATION

反应方程式

HRID 1004437 的结构方程式

REACTANTS

反应物

2
结构：CO
HCID887

Methanol

CH4O

结构：CC(C)(C)c1cc(CO)cc(C(C)(C)C)c1O
HCID6929

2,6-Di-tert-butyl-4-(hydroxymethyl)phenol

C15H24O2

PRODUCTS

生成物

1
结构：COCc1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1
HCID6911

Ethyl 762

C16H26O2

收率 94%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
催化剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

A solution of 4-hydroxymethyl-2,6-di-t-butylphenol (0.5 g) in methanol (10 mL) containing 1 drop of concentrated hydrochloric acid was stirred at ambient temperature for 1 hour. Evaporation of the solvent gave the title compound, 0.5 g, 94% yield as a white crystalline solid.

WORKUP

后处理

  1. customEvaporation of the solvent