Hydrogen Bromide → 2-Benzyl benzylbromide

HRID 1006011

反応式

HRID 1006011 の反応式
[CH2:1]([C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10]O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[BrH:16]>>[CH2:1]([C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10][Br:16])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

3

反応物 2

HCID 260Hydrogen BromideHCID 741092-Benzylbenzyl alcohol

生成物 1

HCID 124220982-Benzyl benzylbromide収率 98%

実験手順

2-Benzylbenzyl alcohol (commercial) (1 g) was suspended in 48% aqueous hydrobromic acid (10 ml) and stirred vigorously for 20 hours. The resultant suspended solid was extracted twice with hexane and the extracts dried (MgSO4) and evaporated to give 2-benzyl benzylbromide as yellow solid (1.3 g, 98%).

後処理

  1. extractionwas extracted twice with hexane
  2. dry with materialthe extracts dried (MgSO4)
  3. customevaporated

出典と根拠

ORDレコード
ord-6a78670be9bd419cb9dfa46ff2da2c77
出典データセット
uspto-grants-2004_09
特許番号
US06787562B2

関連ノート

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