関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Trichloroacetonitrile | HCID 11011 | — |
| 反応物 | Aluminum bromide | HCID 24409 | — |
| 反応物 | 3-[(4-Cyanophenyl)sulfanyl]propanoic acid | HCID 22666602 | — |
| 生成物 | 3-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}propionic Acid | HCID 60111243 | — |
反応手順
The reaction mixture of 22 g of 3-(4-cyanophenyl thio)propionic acid, 150 g of trichloroacetonitrile, and 2 g of AlBr3 was heated to 60° C. in order to dissolve the initially undissolved starting materials, and was bubbled by dry HCl at room temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06797739B1 |
|---|
| 出典データセット | uspto-grants-2004_09 |
|---|
| ORD ID | ord-55159e626f014794ad064a59718bac78 |
|---|
| 出典メモ | uspto-grants-2004_09 |
|---|
