Methyl chloroacetate → HCID 85706506、化合物
反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[Cl:10])[CH:5]=[O:6].Cl[CH2:12][C:13]([O:15][CH3:16])=[O:14].C[O-].[Na+].CO>CO>[Cl:1][C:2]1[CH:3]=[C:4]([CH:5]2[O:6][CH:12]2[C:13]([O:15][CH3:16])=[O:14])[CH:7]=[CH:8][C:9]=1[Cl:10]参加物
5
実験手順
To a solution of 3,4-dichlorobenzaldehyde (51.0 g) and methyl chloroacetate (51 mL) in methanol (500 mL) was added 28% sodium methoxide/methanol (68 mL) solution under ice-cooling, and the mixture was stirred at room temperature overnight. The resultant product was collected by filtration, and washed with distilled water to give the title compound (90.9 g).
後処理
- temperaturecooling
- filtrationThe resultant product was collected by filtration
- washwashed with distilled water
出典と根拠
- ORDレコード
- ord-320308a3e3694e529aef9ab12a06f3f3
- 出典データセット
- uspto-grants-2014_05
- 特許番号
- US08722662B2
反応ノート
読み込み中…