Benzoic anhydride → Benzoic Acid
反応式
[C:1]([O:9]C(=O)C1C=CC=CC=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C1C2=C3C(=CC=C2)C=CC=C3C=1>C(#N)C>[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
4
実験手順
All reactions were run on a 10 mL scale at room temperature for a total of 5.00 min. The benzoic anhydride and internal standard were added from a stock solution which was 1.0M benzoic anhydride and 25,000 pm acenaphthylene in 100% acetonitrile. A total of 5.0 μL of this stock was used (yielding a 1:2000 dilution) to make each reaction 0.5 mM benzoic anhydride and 25 ppm acenaphthylene. Benzoic acid produced was measured by HPLC (high pressure liquid chromatography) using the acenaphthylene internal standard as a reference.
後処理
- customwere run on a 10 mL scale at room temperature for a total of 5.00 min
- customyielding a 1:2000 dilution)
出典と根拠
- ORDレコード
- ord-ff17610db45246418b847043e928669d
- 出典データセット
- uspto-grants-1994_05
- 特許番号
- US05308529
反応ノート
読み込み中…