Benzoic anhydride → Benzoic Acid

HRID 1032867

反応式

HRID 1032867 の反応式
[C:1]([O:9]C(=O)C1C=CC=CC=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C1C2=C3C(=CC=C2)C=CC=C3C=1>C(#N)C>[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

4

反応物 2

HCID 7167Benzoic anhydride3 回HCID 9161Acenaphthylene2 回

生成物 1

HCID 243Benzoic Acid

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

All reactions were run on a 10 mL scale at room temperature for a total of 5.00 min. The benzoic anhydride and internal standard were added from a stock solution which was 1.0M benzoic anhydride and 25,000 pm acenaphthylene in 100% acetonitrile. A total of 5.0 μL of this stock was used (yielding a 1:2000 dilution) to make each reaction 0.5 mM benzoic anhydride and 25 ppm acenaphthylene. Benzoic acid produced was measured by HPLC (high pressure liquid chromatography) using the acenaphthylene internal standard as a reference.

後処理

  1. customwere run on a 10 mL scale at room temperature for a total of 5.00 min
  2. customyielding a 1:2000 dilution)

出典と根拠

ORDレコード
ord-ff17610db45246418b847043e928669d
出典データセット
uspto-grants-1994_05
特許番号
US05308529

関連ノート

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