Allyl bromide → 3-allyl-5-methylthiazol-2(3H)-imine hydrobromide
反応式
[NH2:1][C:2]1[S:3][C:4]([CH3:7])=[CH:5][N:6]=1.[CH2:8]([Br:11])[CH:9]=[CH2:10]>>[BrH:11].[CH2:10]([N:6]1[CH:5]=[C:4]([CH3:7])[S:3][C:2]1=[NH:1])[CH:9]=[CH2:8]参加物
3
実験手順
A mixture of 2-amino-5-methylthiazole (2.5 g) and allylbromide (3.31 g) was processed according to the method of Example 227A to afford the title compound that was taken directly to the next step. MS (ESI+) m/z 155 (M+H)+.
出典と根拠
- ORDレコード
- ord-0246485785de45bfad61e1a05e53d620
- 出典データセット
- uspto-grants-2013_10
- 特許番号
- US08546583B2
反応ノート
読み込み中…